聚苯胺微粒的制备与表征

齐永晓; 赵玉增; 杨瑾妮

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上海电力大学学报:2009,25(5):517-520

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聚苯胺微粒的制备与表征

齐永晓, 赵玉增, 杨瑾妮

(上海电力学院能源与环境工程学院上海 200090)

Preparation and Characterization of Polyaniline Microparticles

QI Yong-xiao, ZHAO Yu-zeng, YANG Jin-ni

(School of Thermal Power and Environmental Engineering, Shanghai University of Electric Power, Shanghai 200090, China)

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投稿时间：2009-06-30

中文摘要: 以苯胺为单体,采用乳液聚合的方法合成聚苯胺,对单体引发剂、乳化剂以及溶剂的不同比例做了对比试验.并通过光学显微镜,红外光谱,TG,DTA,循环伏安法对其进行表征.结果表明,在单体:引发剂:乳化剂:溶剂=1:1:1:20定量条件下,常温搅拌12 h制得的聚苯胺产物颗粒较好.

中文关键词: 聚苯胺乳液聚合微粒

Abstract:Polyaniline is prepared by emulsion polymerization with aniline as monomer.Different ratios of monomer,initiator,emulsifier and solvent are composed in the experiments,which would affect the particle of polyaniline.Then the polyaniline products are respectively characterized by optical microscope,FFIR,TG,DTA and cyclic voltammetry,respectively.The results show that the best ratio of monomer,initiator,emulsifier and sdvent is 1:1:1:20 so that better particles are obtained by stirring 12h at room temperature.

keywords: polyaniline emulsion polymerization microparticles

文章编号：20090525 中图分类号： 文献标志码：

基金项目:上海市教育委员会科研项目(07ZZ148)

作者	单位
齐永晓	上海电力学院能源与环境工程学院上海 200090
赵玉增	上海电力学院能源与环境工程学院上海 200090
杨瑾妮	上海电力学院能源与环境工程学院上海 200090

Author Name	Affiliation
QI Yong-xiao	School of Thermal Power and Environmental Engineering, Shanghai University of Electric Power, Shanghai 200090, China
ZHAO Yu-zeng	School of Thermal Power and Environmental Engineering, Shanghai University of Electric Power, Shanghai 200090, China
YANG Jin-ni	School of Thermal Power and Environmental Engineering, Shanghai University of Electric Power, Shanghai 200090, China

引用文本：
齐永晓,赵玉增,杨瑾妮.聚苯胺微粒的制备与表征[J].上海电力大学学报,2009,25(5):517-520.
QI Yong-xiao,ZHAO Yu-zeng,YANG Jin-ni.Preparation and Characterization of Polyaniline Microparticles[J].Journal of Shanghai University of Electric Power,2009,25(5):517-520.