负载型中孔碳气凝胶脱硫剂的制备及其性能评价

杨思源; 田欢; 吴江

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DOI:10.3969/j.issn.1006-4729.2016.01.005

上海电力大学学报:2016,32(1):15-19

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负载型中孔碳气凝胶脱硫剂的制备及其性能评价

杨思源, 田欢, 吴江

(上海电力学院能源与机械工程学院)

Preparation and Performance Evaluation of the Supported Mesoporous Carbon Aerogel Desulfurizer

YANG Siyuan, TIAN Huan, WU Jiang

(School of Energy and Mechanical Engineering, Shanghai University of Electric Power, Shanghai 200090, China)

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本文已被：浏览 1690次下载 1282次
投稿时间：2015-10-10

中文摘要: 通过溶胶-凝胶法制备了碳气凝胶,用浸渍法合成锰基高温脱硫剂.利用N₂吸附/脱附(BET)、扫描电镜(FESEM)的分析手段对脱硫剂进行物相和微观结构的表征,并在固定床反应器中考察了硫化温度、载体、气体组分对其脱硫性能的影响.结果表明,最佳硫化反应温度为850 ℃;脱硫剂在H₂条件下硫容大大降低,在CO条件下脱硫剂硫容无明显变化.

中文关键词: 碳气凝胶锰基脱硫剂溶胶-凝胶法浸渍法

Abstract:The carbon aerogel is made by sol-gel method and the impregnation method is used to synthesize desulfurizer.The desulfurizer is characterized by means of N₂ adsorption/desorption(BET),field-emission scanning electron microscopy(FESEM).The optimum temperature conditions and the influence of textural parameters of carbon aerogels are explored.The results show that the best reaction temperature is 850 ℃;the sulfur capacity greatly reduces under H₂ conditions,and in the CO condition the desulfurizer sulfur content does not change very much.

keywords: carbon aerogel manganese-based sorbent sol-gel method impregnation method

文章编号：20160105 中图分类号： 文献标志码：

基金项目:

作者	单位	E-mail
杨思源	上海电力学院能源与机械工程学院
田欢	上海电力学院能源与机械工程学院
吴江	上海电力学院能源与机械工程学院	wjcfd2002@sina.com

Author Name	Affiliation	E-mail
YANG Siyuan	School of Energy and Mechanical Engineering, Shanghai University of Electric Power, Shanghai 200090, China
TIAN Huan	School of Energy and Mechanical Engineering, Shanghai University of Electric Power, Shanghai 200090, China
WU Jiang	School of Energy and Mechanical Engineering, Shanghai University of Electric Power, Shanghai 200090, China	wjcfd2002@sina.com

引用文本：
杨思源,田欢,吴江.负载型中孔碳气凝胶脱硫剂的制备及其性能评价[J].上海电力大学学报,2016,32(1):15-19.
YANG Siyuan,TIAN Huan,WU Jiang.Preparation and Performance Evaluation of the Supported Mesoporous Carbon Aerogel Desulfurizer[J].Journal of Shanghai University of Electric Power,2016,32(1):15-19.